Journal
ORGANIC LETTERS
Volume 9, Issue 15, Pages 2827-2830Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0710616
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The synthesis of the trisubstituted cyclobutane 7, which is a suitable precursor for the preparation of oxetanocin carbocyclic analogues, is described. The key step involves a regio- and diastereoselective [2 + 2] photochemical reaction of ketene diethyl acetal with (S)-5-pivaloyloxymethyl-2(5H)-furanone, 3. As an application of this methodology, (-)-cyclobut-A has been prepared from the intermediate 7.
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