4.6 Article

Analytical method for the determination of sterigmatocystin in grains using high-performance liquid chromatography-tandem mass spectrometry with electrospray positive ionization

Journal

JOURNAL OF CHROMATOGRAPHY A
Volume 1157, Issue 1-2, Pages 467-471

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ELSEVIER
DOI: 10.1016/j.chroma.2007.05.022

Keywords

sterigmatocystin; mycotoxin; LC-MS-MS; validation; Aspergillus spp.

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A sensitive LC-electrospray positive ionization (ESI+) MS/MS method was developed and validated for the determination of the Aspergillus mycotoxin. sterigmatocystin, in grains at levels down to less than 0.5 mu g/kg. Recovery was found to be greater than 97% for wheat grains. (c) 2007 Elsevier B.V. All rights reserved.

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