Journal
MATERIALS LETTERS
Volume 61, Issue 21, Pages 4332-4335Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2007.01.099
Keywords
tungsten disulfide; solvothermal; hollow spherical; trioctylamine; fullerenes; nanomaterials
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Tungsten disulfide hollow spherical nanoparticles with diameters of about 100 nm modified by trioctylamine (TOA) have been successfully prepared by a solvothermal Process in pyridine. For comparison, WS2 sample was also prepared without TOA modification and sheet-like pieces and their irregular aggregates were obtained. The products were characterized by X-ray power diffraction (XRD), X-ray photoclectron microscopy (XPS), transmission electron microscopy (TEM) and high revolution transmission electron microscopy (HRTEM), respectively. (c) 2007 Elsevier B.V. All rights reserved.
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