Journal
ORGANIC LETTERS
Volume 9, Issue 16, Pages 3145-3148Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol071356j
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[GRAPHICS] Coating of silica-supported sulfonic acid catalysts with hydrophobic ionic liquid leads to a significant improvement of catalyst selectivity. Many organic reactions, including Prins cyclization, cycloaddition of epoxide to aldehyde, and dehydrative etherification of secondary benzyl alcohols, proceed well in formalin or pure water. In particular, tandem dehydration/Prins cyclization reactions of tertiary and secondary alcohols with formaldehyde were developed for the first time.
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