Journal
ANALYTICA CHIMICA ACTA
Volume 806, Issue -, Pages 27-54Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.aca.2013.10.047
Keywords
Ion chromatography; Mass spectrometry; Oxyhalides; Cations; Anions; Explosives
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The development and application of ion chromatography (IC) coupled to mass spectrometry (MS) is discussed herein for the quantitative determination of low-order explosives-related ionic species in environmental and forensic sample types. Issues relating to environmental explosives contamination and the need for more confirmatory IC-MS based applications in forensic science are examined. In particular, the compatibility of a range of IC separation modes with MS detection is summarised along with the analytical challenges that have been overcome to facilitate determinations at the ng-mu g L-1 level. Observed trends in coupling IC to inductively coupled plasma and electrospray ionisation mass spectrometry form a particular focus. This review also includes a discussion of the relative performance of reported IC-MS methods in comparison to orthogonal ion separation-based, spectrometric and spectroscopic approaches to confirmatory detection of low-order explosives. Finally, some promising areas for future research are highlighted and discussed with respect to potential IC-MS applications. (C) 2013 Elsevier B.V. All rights reserved.
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