Journal
TETRAHEDRON LETTERS
Volume 48, Issue 34, Pages 6027-6030Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.06.103
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Primary, secondary, and tertiary alkoxyl radicals add exo-selectively to the olefinic pi-bond in bicyclo[2.2.1]heptene to afford exo-2-alkoxybicyclo[2.2.1]kept-3-yl radicals, which are trapped with BrCCl3 preferentially from the endo face to furnish beta-bromohydrine ethers in 23-67% yield. (c) 2007 Elsevier Ltd. All rights reserved.
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