Journal
ORGANIC LETTERS
Volume 9, Issue 18, Pages 3535-3538Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol071397f
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ZnBr2 was found to catalyze formation of propargyl and propargylic Grignard reagents, and thus put an end to the standard method using a mercury catalyst. The Grignard reagents were submitted to addition reaction with carbonyl compounds and allylation with the cyclic monoacetate to afford the propargyl-type products selectively. Furthermore, the product from the monoacetate was transformed to an acetylene analogue of 2-(5,6-epoxyisoprostane A(2))phosphorylcholines.
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