Journal
JOURNAL OF CLUSTER SCIENCE
Volume 18, Issue 3, Pages 764-771Publisher
SPRINGER/PLENUM PUBLISHERS
DOI: 10.1007/s10876-007-0146-5
Keywords
nanoparticles; selenosulfide; mercury; phosphine
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Mercury-selenosulfide (HgSe (x) S (1-x) ) nanoparticles have been synthesized using the single-source reagent Me3Si-SeS-SiMe3. The reagent distributes Se2- and S2- to the metal core as the reaction between Me3Si-SeS-SiMe3 and mercury acetate occurs via a redox pathway, ultimately giving rise to Se-S bond cleavage. Particles are characterized by EDX, TEM and powder X-ray diffraction analysis in conjunction with UV-Visible absorption spectroscopy.
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