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A critical review in calibration methods for solid-phase microextraction

Journal

ANALYTICA CHIMICA ACTA
Volume 627, Issue 2, Pages 184-197

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.aca.2008.08.015

Keywords

Solid-phase microextraction; Traditional calibration; Equilibrium extraction; Exhaustive extraction; Diffusion-based calibration

Funding

  1. Guangdong Provincial Key Laboratory of Environmental Pollution Control and Remediation Technology
  2. Natural Sciences and Engineering Research Council of Canada

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Solid-phase microextraction (SPME) was developed to address the need for rapid sampling and sample preparation, both in the laboratory and on-site. Unlike traditional sample preparation methods, SPME is a non-exhaustive extraction technique in which only a small portion of the target analyte is removed from the sample matrix. Therefore, calibration of SPME for quantitative analysis is very important. in this review, we summarized the proposed SPME calibration methods and the characteristics of these methods were discussed. (C) 2008 Elsevier B.V. All rights reserved.

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