Journal
TRANSITION METAL CHEMISTRY
Volume 32, Issue 6, Pages 711-715Publisher
SPRINGER
DOI: 10.1007/s11243-007-0234-2
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A novel dinuclear nickel(II) complex, [Ni-2(MOBPT)(2)Cl-2(H2O)(2)]Cl-2 center dot 7H(2)O (MOBPT = 4-(p-methoxyphenyl) -3,5-bis(pyridine-2-yl)-1,2,4-triazole), has been synthesized and characterized by elemental analysis, IR and single crystal X-ray diffraction methods. The crystal structure determination shows that the dinuclear Ni2N8 unit is almost planer in which each Ni-II stop ion is coordinated by four nitrogen atoms from MOBPT equatorially and a water molecule and a chloride ion axially in a distorted octahedral geometry. Magnetic measurements reveal a relatively weak antiferromagnetic exchange in the complex.
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