Journal
JOURNAL OF SYNCHROTRON RADIATION
Volume 14, Issue -, Pages 395-402Publisher
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S0909049507029962
Keywords
three-dimensional chemical imaging; scanning transmission X-ray microscopy; NEXAFS spectroscopy; polystyrene microspheres; polyacrylates; tomography
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Three-dimensional (3-d) chemical mapping using angle-scan tomography in a scanning transmission X-ray microscope is demonstrated. Apparatus, experimental procedures and data processing are presented and the 3-d spatial resolution is evaluated. The technique is illustrated using mapping of a low-density acrylate polyelectrolyte in and outside of polystyrene microspheres dispersed in water in a 4 mu m-diameter microcapillary. The 3-d chemical visualization provides information about the microstructure that had not previously been observed.
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