Journal
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING
Volume 89, Issue 1, Pages 77-80Publisher
SPRINGER
DOI: 10.1007/s00339-007-4073-y
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Litharge, the red tetragonal form of lead oxide alpha-PbO and massicot, the yellow orthorhombic form beta-PbO, are synthesized from lead(II) salts in aqueous media at elevated temperatures. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to characterize the size, morphology, and crystallographic structural forms of the products. The role of impurities in the experimental synthesis of the materials and microstructural variations in the final products are described. The implications of these observations regarding the synthesis of different conducting lead oxides and other related materials are discussed.
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