4.2 Article

Preparation and characterization of some keto-bile acid azines

Journal

STEROIDS
Volume 72, Issue 11-12, Pages 756-764

Publisher

ELSEVIER SCIENCE INC
DOI: 10.1016/j.steroids.2007.06.005

Keywords

steroids; dimeric bile acids; homo- and heteroazines; synthesis

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New acyclic dimers of ketocholanic acids with hydrazine were obtained. Crystal structure was determined for the 3,7-dihydroxy-12-ketocholanic acid azine. Some distinctive H-1 NMR signals are assigned for the entire set of azines. (c) 2007 Elsevier Inc. All rights reserved.

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