Journal
ORGANIC LETTERS
Volume 9, Issue 22, Pages 4555-4557Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol7020077
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[GRAPHICS] The conformational preferences of ethanolamine and its hydrochloride in solution were estimated by comparing experimental NMR vicinal proton-proton coupling constants to semiemprical coupling constants for each staggered rotamer, derived by the Haasnoot-Altona method. Strong gauche preferences are observed for both ethanolamine and its hydrochloride over a wide range of solvent polarities. Concentration was not observed to significantly affect the position of the conformer equilibria.
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