Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 72, Issue 22, Pages 8416-8421Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo701590p
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A new structural phenanthroindolizidine, 2,3,6,7-tetramethoxyphenanthro[9,10,3('),4(')]indolizidine, has been synthesized efficiently from pyrrole. An important feature of this synthesis is that intramolecular oxidative coupling and rearrangement of 6,7-bis(3,4-dimethoxyphenyl)-8-methoxy-1,2,3-trihydroindolizin-5-one by using VOF3 and TFA have been achieved in one pot.
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