Journal
CHEMISTRY OF MATERIALS
Volume 19, Issue 22, Pages 5373-5376Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm071370q
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We report the first successful synthesis of TiO2(B) nanoparticles by a one-step hydrothermal process. The process was performed under acidic conditions in a 0.59 M H2SO4 solution at 160 degrees C for 24 h or at 200 degrees C for 6 h using a titanium metal complex with glycolic acid. The prepared nanoparticles were characterized by XRD, Raman spectroscopy, and TEM. TiO2(B) is a metastable phase and is one of the most intriguing forms of titanium oxide. All synthesis methods for TiO2(13) reported to date have required a. multistep process involving solid-state synthesis of an alkali metal titanate, an ion-exchange reaction, and gentle dehydration.
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