Journal
TETRAHEDRON LETTERS
Volume 48, Issue 46, Pages 8108-8110Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.09.114
Keywords
regioselective; Suzuki coupling; thiophenes; one-pot; dehalogenation
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Funding
- NIGMS NIH HHS [R15 GM074662-01, R15 GM074662] Funding Source: Medline
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Conditions have been identified that enable the one-pot double Suzuki coupling of 4,5-dibromothiophene-2-carboxaldehyde to proceed in good yield. The key to success in these reactions is the use of minimal amounts of water to avoid significant amounts of dehalogenation during the first coupling. (c) 2007 Elsevier Ltd. All rights reserved.
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