Journal
ORGANIC LETTERS
Volume 9, Issue 24, Pages 5051-5054Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol702255k
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Funding
- NIGMS NIH HHS [R01 GM067726-05, R01 GM067726] Funding Source: Medline
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The BC ring system of upenamide was assembled using a stereoselective Diels-Alder reaction followed by a Staudinger/aza-Wittig/imine hydrolysis reaction. Stereoselective aldol coupling with an aldehyde that incorporates the DE ring system led to an advanced. synthetic intermediate en route to the marine alkaloid upenamide.
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