Journal
ORGANIC LETTERS
Volume 9, Issue 25, Pages 5159-5162Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol7020803
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(Me3Si)(3)SiH was used as a successful reagent in a variety of radical-based transformations in water. The system comprising substrate, silane, and initiator (ACCN) mixed in aqueous medium at 100 degrees C worked well for both hydrophilic and hydrophobic substrates, with the only variation that an amphiphilic thiol was also needed in case of the water-soluble compounds.
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