Journal
TETRAHEDRON LETTERS
Volume 48, Issue 50, Pages 8922-8925Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.10.041
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Ketone zincate-type enolates can be applied to radical trifluoromethylation for the general synthesis of alpha-CF3-ketones, cyclopentanones in particular. The addition of diethylzinc to lithium enolates is the key in the preparation of the zincate-type enolates for efficient radical trifluoromethylation. (c) 2007 Elsevier Ltd. All rights reserved.
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