Journal
ORGANIC LETTERS
Volume 9, Issue 26, Pages 5349-5352Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol7025284
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Funding
- NIGMS NIH HHS [R01 GM046503, GM 46503, R01 GM046503-12, R37 GM046503] Funding Source: Medline
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Dirhodium caprolactamate is the most efficient catalyst for the oxidation of Delta(5)-steroids to 7-keto-Delta(5)-steroids by 70% tert-butyl hydroperoxide in water (T-HYDRO). Isolated product yields range from 38 to 87%.
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