Journal
TETRAHEDRON LETTERS
Volume 48, Issue 52, Pages 9176-9179Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.10.106
Keywords
reduction; sulfoxides; dioxomolybdenum dichloride; boranes; B-H activation
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The first example of an organic reduction with boranes catalyzed by a high valent oxo-complex is reported. The systems catecholborane/MoO2Cl2(H2O)(2) and BH3 center dot THF/MoO2Cl2 (5 mol %) proved to be very efficient for the reduction of sulfoxides to the corresponding sulfides in excellent yields. (c) 2007 Elsevier Ltd. All rights reserved.
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