Journal
INTERNATIONAL JOURNAL OF APPLIED CERAMIC TECHNOLOGY
Volume 12, Issue -, Pages E111-E120Publisher
WILEY
DOI: 10.1111/ijac.12382
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Funding
- Recruitment Program of Global Youth Experts of Sichuan Province
- Youth Hundred Talents Project of Sichuan Province
- National Natural Science Foundation of China [51202203, 91326102]
- China Postdoctoral Science Foundation [2012M520078, 2013T60861]
- Southwest University of Science and Technology [13zx9108]
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Synroc is recognized as the second generation waste form for the disposal of high-level radioactive waste (HLW). In this research, one of the mostly studied Synroc minerals, zirconolite (CaZrTi2O7), was prepared by self-propagating high-temperature synthesis (SHS). CuO and MoO3 were employed as the oxidants with Ti as the reductant. Different TiO2/Ti ratios were selected to investigate reactivity and adiabatic temperature (T-ad) of the designed SHS reactions. Zirconolite was successfully synthesized as the main phase at varied TiO2/Ti ratios using CuO and MoO3 as the oxidants. The as-synthesized samples were readily solidified with desirable density and Vickers hardness.
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