Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 360, Issue 8, Pages 1665-1672Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201701536
Keywords
Electrochemical oxidative amination; C-N formation; Ferrocene; Redox mediator
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Funding
- National Key Technology RD Program [2011BAD23B01, 2017YFB0307502]
- National Natural Science Foundation of China [21472011]
- Open Project Program of Beijing Key Laboratory of Flavor Chemistry, Beijing Technology and Business University (BTBU)
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Efficient intermolecular dehydrogenative cross-coupling of N-alkyloxyamides with xanthenes is reported. The protocol is carried out in an undivided cell under constant current conditions employing simple, cheap and readily available ferrocene (Fc) as a redox catalyst. Cyclic voltammetry and control experiments disclosed that the dehydrogenative cross-coupling reaction may proceed via an amidyl radical.
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