Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 356, Issue 5, Pages 1038-1046Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201300895
Keywords
CH activation; oxidative olefination; pyridines; rhodium
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Funding
- National Science Foundation of China [21002087, 21272206, J1210042]
- Fundamental Research Funds for the Central Universities [2010QNA3033]
- Zhejiang Provincial NSFC [Z12B02000]
- Qianjiang Project [2013R10033]
- Ministry of Education [SRFDP 20110101110005]
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A rhodium(III)-catalyzed selective olefination of picolinamide derivatives has been developed. The reaction shows high regioselectivity, low catalyst loading (0.5mol%), high yield and good functional group tolerance, providing a convenient strategy for the synthesis of 3-alkenylpicolinamides.
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