Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 356, Issue 13, Pages 2801-2806Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201400290
Keywords
multi-component reactions (MCR); oxidation; photocatalysis; photosynthesis; 2-pyrimidinethiones; thioureas
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Funding
- National Natural Science Foundation of China [21172023]
- Applied Basic Research Plan of Changzhou [CJ20120029]
- Priority Academic Program Development (PAPD) of Jiangsu Higher Education Institutions
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A photo-assisted metal-free multi-component dehydrogenative condensation has been developed. This multi-component reaction (MCR) has been realized under mild reaction conditions especially under household light irradiation. As a result, the novel tetrahydropyrimidines (THPMs) were obtained in moderate yields and excellent stereoselectivities. Moreover, the approach provided an easy construction of a variety of 2-pyrimidinethiones from the commonly used cyclic ethers.
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