Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 355, Issue 4, Pages 809-813Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201200874
Keywords
beta-amidovinyl sulfones; C-H activation; iridium; photochemistry; redox chemistry
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Funding
- National Basic Research Program of China [2011CB935800]
- National Natural Science Foundation of China [2112109, 21102072]
- Natural Science Foundation of Jiangsu Province [BK2012012]
- State Key Laboratory of Bioorganic & Natural Products Chemistry, Shanghai Institute of Organic Chemistry, CAS
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A mild, practical and environmentally friendly strategy to prepare -amidovinyl sulfones has been developed based on the sulfonation of enamides or enecarbamates via visible-light photoredox catalysis. Direct CH functionalizations of enamides or enecarbamates under the optimized conditions proceeded with a wide scope of substrates and remarkable selectivity to give functionalized vinyl sulfones with good to excellent yields.
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