Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 354, Issue 18, Pages 3551-3560Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201200624
Keywords
C?C coupling; green chemistry; polymers; recycling; Stille reaction; tin
Categories
Funding
- Spanish MEC (DGI) [CTQ2010-18901/BQU]
- Junta de Castilla y Leon [VA373A11-2]
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The Stille coupling can be carried out in a batch process using insoluble tin supports. The new type of support consists of stannylated polymers based on the vinylic polynorbornene skeleton that allow one to use a set-up where the tin reagent is immobilized in a column. The immobilized stannylated polymeric reagent can be easily reused. The coupling products are thus obtained by a very simple work-up procedure and have very low levels of tin contamination.
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