Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 351, Issue 14-15, Pages 2369-2378Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200900358
Keywords
aryl-sulfur bond; cross-coupling; heterogeneous catalyst; recycling; unsymmetrical organic sulfides
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Funding
- DST, New Delhi [SR/S2/JCB-11/2008]
- CSIR, New Delhi
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Alumina-supported copper sulfate efficiently catalyzes the S-arylation of aromatic, heteroaromatic and aliphatic thiols with aryl as well as heteroaryl halides under aerobic, ligand-free conditions. This protocol provides an easy access to a variety of thioethers as well as unsymmetrical bis-thioethers by base-controlled differential coupling of thiols with iodo- and bromo-substituents in an aromatic halide. The catalyst is inexpensive, non-air sensitive, environmentally friendly and recyclable.
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