Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 350, Issue 13, Pages 1949-1953Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200800211
Keywords
heterogeneous catalysis; immobilization; metathesis; N-heterocyclic carbenes; ring-opening polymerization; ruthenium
Categories
Funding
- IAP-PAI
- IDECAT
- GOA
- CECA T scheme
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The second generation Hoveyda-Grubbs metathesis catalyst was successfully immobilized on silica in pellet and powder form following a practical and fast synthesis procedure. The activity of the solid system is truly heterogeneous, efficient in various metathesis reaction types and stable for at least 4000 TON. Ru contamination of the products was very low (ppb levels). The successful use of the robust system has been demonstrated in a continuous reactor set-up.
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