Journal
INORGANIC MATERIALS
Volume 51, Issue 9, Pages 891-896Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0020168515090150
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Funding
- Russian Foundation for Basic Research [13-03-00662]
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Using thermogravimetry, differential scanning calorimetry, X-ray diffraction, mass spectrometry, and Fourier transform IR spectroscopy, we have determined the composition of VO(acac)(2) thermal decomposition products and gained insight into the bond breaking sequence in this compound. A two-step annealing procedure has been proposed to ensure control over VO(acac)(2) to VO2 conversion processes without changing the oxidation state of vanadium in the preparation of VO2 films by a sol-gel process.
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