Journal
ACTA MATERIALIA
Volume 56, Issue 14, Pages 3380-3393Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.actamat.2008.03.032
Keywords
in situ transmission electron microscopy (TEM); grain-boundary migration; nanocrystalline film; aluminum
Funding
- NSF NIRT Program [DMR-0210215]
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Free-standing nanocrystalline Al thin films have been strained in situ in a transmission electron microscope at room-temperature. Extensive grain-boundary migration accompanies the in situ loading and has been observed to occur preferentially at crack tips and only in the presence of the applied stress. This grain growth precedes dislocation activity, and measured boundary velocities are greater than can be explained by diffusive processes. The unambiguous observations of stress-assisted grain growth are compatible with recently proposed models for stress-coupled grain-boundary migration. The growth occurs in a faceted manner indicative of preferential boundaries. The fast collapse of small grains with sizes of 30-50 nm demonstrates the unstable nature of a nanocrystalline structure. Clearly observable shape changes testify to the effectiveness of grain-boundary migration as a deformation mechanism, and preferential grain growth at crack tips resulted in efficient crack tip blunting, which is expected to improve the films' fracture toughness. (c) 2008 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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