Journal
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Volume 70, Issue -, Pages O1128-+Publisher
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600536814020911
Keywords
crystal structure; hydrogen bonds; 1,2,3-triazole
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Funding
- NIH/National Cancer Institute, United States [CA140409]
- Arkansas Research Alliance
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The title compound, C20H23N3O6 center dot CH3OH was synthesized by [3 + 2] cycloaddition of (Z)-2,3-bis(3,4,5-trimethoxyphenyl)-acrylonitrile with sodium azide and ammonium chloride in DMF/water. The central nitrogen of the triazole ring is protonated. The dihedral angles between the triazole ring and the 3,4,5-trimethoxyphenyl ring planes are 34.31 (4) and 45.03 (5)degrees, while that between the 3,4,5-trimethoxyphenyl rings is 51.87 (5)degrees. In the crystal, the molecules, along with two methanol solvent molecules are linked into an R-4(4)(10) centrosymmetric dimer by N-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds.
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