Journal
ACS SUSTAINABLE CHEMISTRY & ENGINEERING
Volume 6, Issue 4, Pages 4916-4921Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acssuschemeng.7b04400
Keywords
Oxidation; Aldehyde; Carboxylic acid; Acid anhydride; Air
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Funding
- National Natural Science Foundation of China [21302048, 21273068, 21545010]
- Scientific Research Hunan Provincial Education Department [15C0464]
- Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province [2012-318]
- Construct Program of the Key Discipline in Hunan Province
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An economic, safe, practical, and environmentally benign protocol for the oxidation of aldehydes to carboxylic acids and acid anhydrides with ambient air as the sole oxidant was developed. This oxidation is operationally simple and external catalyst-, initiator-, and base-free, with outstanding functional group tolerance (moisture-, acid-, base-, and oxidant-sensitive groups). It also provides a practical protocol for large scale synthesis (>100 g), late-stage modification of polyfunctional compounds, and one-pot sequential transformation starting from aldehydes.
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