4.4 Article

Optimization of monochromated TEM for ultimate resolution imaging and ultrahigh resolution electron energy loss spectroscopy

Journal

ULTRAMICROSCOPY
Volume 184, Issue -, Pages 109-115

Publisher

ELSEVIER
DOI: 10.1016/j.ultramic.2017.08.016

Keywords

EELS; Ultra-low energy loss; Phonons; Plasmons; Bandgap; Sub-angstrom resolution

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The performance of a monochromated transmission electron microscope with Wien type monochromator is optimized to achieve an extremely narrow energy spread of electron beam and an ultrahigh energy resolution with spectroscopy. The energy spread in the beam is improved by almost an order of magnitude as compared to specified values. The optimization involves both the monochromator and the electron energy loss detection system. We demonstrate boosted capability of optimized systems with respect to ultra-low loss EELS and sub-angstrom resolution imaging (in a combination with spherical aberration correction). (C) 2017 Elsevier B.V. All rights reserved.

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