4.7 Article

TiO2 anti-corrosive thin films on duplex stainless steel grown using cathodic cage plasma deposition

Journal

SURFACE & COATINGS TECHNOLOGY
Volume 347, Issue -, Pages 136-141

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.surfcoat.2018.04.074

Keywords

TiO2; Cathodic cage plasma deposition; Thin film; Corrosion

Funding

  1. PPGEM-IFPI
  2. CAPES
  3. FAPEPI
  4. CNPq [303752/2017-3, 304133/2017-5]
  5. Universidade Brasil [303752/2017-3, 304133/2017-5]

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Herein, we evaluated the influence of different experimental parameters to obtain high anti-corrosive anatase TiO2 thin films on stainless steel using a simple and low cost cathodic cage plasma deposition technique at low pressure and temperature. The thin TiO2 films were deposited on duplex stainless-steel (dimension). Different mixtures of O-2, H-2 and Ar were used and further correlated with resulting structural properties and corrosion resistance. The temperature was kept at 450 degrees C with a deposition time from 1 to 4 h. Raman spectroscopy, grazing incidence X-ray diffraction and a corrosion test were used to evaluate the TiO2 films. A thin TiO2 adherent, crystalline, protective film was obtained when 60% H-2/40% Ar was used. Our proposed method to obtain TiO2 films shows promise for use in different industrial applications.

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