Journal
PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES
Volume 101, Issue -, Pages 284-293Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.physe.2018.04.017
Keywords
Humidity; Porosity; KIT-6; Sensors; Ia(3)over-bard symmetry
Funding
- Council of Scientific and Industrial Research (CSIR) New Delhi-INDIA [03/(1377)/16/EMR-II]
- University Grant Commissions (UGC) [2061510043]
- CSIR, New Delhi [03/(1377)/16/EMR-II]
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The present scientific investigation deals with template synthesis of 3D-cubic mesoporous KIT-6 with in-situ loading of SnO2 to obtain a material with enhanced number of surface active sites. The structural insights have been reported through analysis of XRD, TEM, FESEM, N-2 sorption and mid-IR absorption data. X-ray diffraction confirmed 3D-cubic mesoporous structure of silica with Ia(3)over-bard symmetry and existence of anatase SnO2 species. A decrease in surface area on loading of SnO2 nanoparticles is revealed via analysis of N-2 adsorption-desorption isotherms. Rapid response time of 15 s and super rapid recovery time of 2 s (with response > 100) have been exhibited by sensor based on sample containing 1 wt% of SnO2 . Further investigation on sensing performance of nanocomposite with 1 wt% of SnO2 confirmed its ohmic behavior (with negligible V-I hysteresis), excellent cycle stability, outstanding long term stability and very low hysteresis (1.4% at 53% RH).
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