Journal
ORGANIC LETTERS
Volume 20, Issue 8, Pages 2156-2159Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b00391
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A simplified approach to quantum yield (phi) measurement using in situ LED NMR spectroscopy has been developed. The utility and performance of NMR actinometry has been demonstrated for the well-known chemical actinometers potassium ferrioxalate and o-nitrobenzaldehyde. A novel NMR-friendly actinometer, 2,4-dinitrobenzaldehyde, has been introduced for both 365 and 440 nm wavelengths. The method has been utilized successfully to measure the quantum yield of several recently published photochemical reactions.
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