Journal
ORGANIC LETTERS
Volume 20, Issue 13, Pages 3996-3999Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b01563
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Funding
- National Natural Science Foundation of China [21425415, 21774056]
- National Basic Research Program of China [2015CB856303]
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A Rh(III)-catalyzed enaminone-directed alkenyl C-H coupling with alkynes for the synthesis of salicylaldehyde derivatives is reported. This represents a unique example of benzene ring framework formation through a transition-metal-catalyzed, directed C-H activation strategy. The two incorporated reactive functionalities, aldehyde and hydroxy groups, provide convenient synthetic handles for further structural elaboration.
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