Journal
ORGANIC LETTERS
Volume 20, Issue 12, Pages 3527-3530Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b01294
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Funding
- National Natural Science Foundation of China [21562005, 21602037]
- Natural Science Foundation of Guangxi [2015GXNSFCA139001, 2016GXNSFFA380005]
- Ministry of Education of China [IRT_16R15]
- Overseas 100 Talents Program of Guangxi Higher Education
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A variety of 2-aminobenzonitriles were prepared from 2-arylindoles in good to excellent yields through tert-butylnitrite (TBN)-mediated nitrosation and sequential iron(III)-catalyzed C-C Bond cleavage in a one-pot fashion. The 2-aminobenzonitriles can be used to rapidly synthesize benzoxazinones by intramolecular condensation. The present method features an inexpensive iron(III) catalyst, gram scalable preparations, and novel C-C bond cleavage of indoles.
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