Journal
ORGANIC LETTERS
Volume 20, Issue 3, Pages 740-743Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b03881
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Funding
- NSFC [21525208, 21472186]
- new technology of methanol conversion of Dalian Institute of Chemical Physics (Chinese Academy of Sciences)
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Rhodium(Ill)-catalyzed C-H activation of (hetero)arenes and redox-neutral coupling with 2-carboxyl allylic alcohols has been realized for the construction of beta-aryl ketones. This reaction occurred efficiently at a relatively low catalyst loading via initial dehydrogenative alkylation to give a beta-keto carboxylic acid, followed by decarboxylation.
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