Journal
ORGANIC LETTERS
Volume 20, Issue 3, Pages 836-839Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b03986
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Funding
- Al Jalila Foundation, UAE [AJF201531]
- Research Funding Department, University of Sharjah-UAE [15011101007, 15011101002]
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Employing a build/couple/pair strategy, a serendipitous one-pot protocol for the diastereoselective construction of diverse collections of chromenopyrroles is described. This methodology features an unprecedented five-step cascade including azomethine ylide generation followed by in situ intramolecular [3 + 2]-cycloaddition. Furthermore, this protocol was extended to access enantiopure chromenopyrroles using amino acids as chiral auxiliary. Moreover, postpairing reactions were employed to increase the diversity and complexity of our pilot compound collections.
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