4.8 Article

Electrosynthesis of Trisubstituted 2-Oxazolines via Dehydrogenative Cyclization of β-Amino Arylketones

Journal

ORGANIC LETTERS
Volume 20, Issue 9, Pages 2505-2508

Publisher

AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b00165

Keywords

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Funding

  1. Natural Science Foundation of China [U1504208, 21602119, 21702113, 21702013]
  2. China Postdoctoral Science Foundation
  3. Fundamental Research Funds from the Central Universities [buctrc201721, PYCC1707]

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An electrochemically intramolecular functionalization of C-(sp(3))-H bonds with masked oxygen nucleophiles was developed. With IU as the catalyst and electrolyte, diverse trisubstituted 2-oxazolines were constructed in good to excellent yields. This newly developed electrochemical dehydrogenalive approach features external oxidant-free and additive-free conditions.

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