Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 16, Issue 10, Pages 1713-1719Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8ob00244d
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Funding
- Science and Technology Planning Project of Guangdong Province [2015A020211026, 2017A010103044]
- 100 Young Talents Programme of Guangdong University of Technology [220413506]
- Key Laboratory of Functional Molecular Engineering of Guangdong Province (South China University of Technology) [2016kf07]
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A highly efficient sulfonylation of thiols has been achieved through the metal-free NaI/TBHP-mediated cross-coupling of sulfonyl hydrazides and thiols at room temperature. This method provides a convenient and practical route to thiosulfonates in 84-99% yields (39 examples) with wide functional group compatibility.
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