Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 16, Issue 22, Pages 4086-4089Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8ob00877a
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Funding
- Science and Technology Planning Project of Guangdong Province [2015A020211026, 2017A010103044]
- Natural Science Foundation of Guangdong Province [2017A030313071]
- 100 Young Talents Programme of Guangdong University of Technology [220413506]
- Open Fund of the Key Laboratory of Functional Molecular Engineering of Guangdong Province (South China University of Technology) [2016kf07]
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An efficient halogen-free Cs2CO3-promoted methylene insertion into disulfide bonds has been achieved using acetone as a methylene source under mild conditions. This method provides a convenient and practical route to dithioacetals in up to 96% yield with good functional group compatibility.
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