Journal
JOURNAL OF SULFUR CHEMISTRY
Volume 39, Issue 2, Pages 164-172Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/17415993.2017.1405959
Keywords
Ketene dithioacetals; carbon disulfide; arylidenemalononitriles; three-component reaction; active methylene compounds
Categories
Ask authors/readers for more resources
An efficient and simple method for the synthesis of novel ketene dithioacetals via a one-pot three-component reaction of 5,5-dimethylcyclohexan-1,3-dion or 1,3-cyclohexandion with carbon disulfide in the presence of arylidenemalononitriles is reported. The effects of different bases have been investigated and triethylamine can provide products in good to excellent yields at room temperature. The structures of all the synthesized compounds were established from advanced spectroscopic data. [GRAPHICS] .
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available