Journal
JOURNAL OF SEPARATION SCIENCE
Volume 41, Issue 9, Pages 1995-2002Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201701156
Keywords
environmental analysis; gas chromatography; polycyclic aromatic hydrocarbons; silicon carbide; solidphase microextraction
Categories
Funding
- Shandong Provincial Natural Science Foundation of China [ZR2017MB043]
- National Natural Science Foundation of China (NSFC) [21777054]
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Silicon carbide has excellent properties, such as corrosion resistance, high strength, oxidation resistance, high temperature, and so on. Based on these properties, silicon carbide was coated on stainless-steel wire and used as a solid-phase microextraction coating, and polycyclic aromatic hydrocarbons were employed as model analytes. Using gas chromatography, some important factors that affect the extraction efficiency were optimized one by one, and an analytical method was established. The analytical method showed wide linear ranges (0.1-30, 0.03-30, and 0.01-30 mu g/L) with satisfactory correlation coefficients (0.9922-0.9966) and low detection limits (0.003-0.03 mu g/L). To investigate the practical application of the method, rainwater and cigarette ash aqueous solution were collected as real samples for extraction and detection. The results indicate that silicon carbide has excellent application in the field of solid-phase microextraction.
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