Journal
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
Volume 18, Issue 1, Pages 591-603Publisher
AMER SCIENTIFIC PUBLISHERS
DOI: 10.1166/jnn.2018.13922
Keywords
Nano Bronsted Acidic Catalyst; N-Sulfonic Acids; 2H-Indazolo[2,1-b]Phthalazine-1,6,11(13H)-Triones; Solvent-Free Conditions
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Funding
- Guilan University Research Council
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In this research work, 4,4'-(butane-1,4-diyl) bis(1-sulfo-1,4-diazabicyclo[2.2.2]octane-1,4-diium) tetrachloride (NS-C4(DABCO-SO3H)(2)center dot 4Cl) as a new nano-sized N-sulfonic acid was prepared and characterized using different types of spectroscopic methods including FT-IR, H-1 NMR, C-13 NMR, XRD, TGA and SEM analysis. This new reagent was efficiently used as catalyst for the promotion of the one-pot synthesis of 2H-indazolo[2,1-b] phthalazine-1,6,11(13H)-triones derivatives, as a class of biologically active compounds with important pharmaceutical properties, under solvent-free conditions during short reaction times in high yields.
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