Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 293, Issue -, Pages 19-27Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2018.05.012
Keywords
Pure shift NMR; Homodecoupling; Band-selective decoupling; NMR
Funding
- Engineering and Physical Sciences Research Council [EP/N033949/1]
- EPSRC [EP/L018500/1, EP/N033949/1] Funding Source: UKRI
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Homonuclear decoupling can give impressive improvements in spectral resolution when overlapping multiplet structures limit the interpretability of NMR spectra. General homodecoupling methods (pure shift NMR) typically use either interferogram-style acquisition, which is slow but gives optimum resolution, or real-time acquisition, which is fast but gives broader lines. Here we describe an alternative data acquisition strategy that allows rapid acquisition without resolution loss, illustrating the method with band-selective homodecoupling experiments and demonstrating its advantages over competing methods. (C) 2018 Elsevier Inc. All rights reserved.
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