Journal
RSC ADVANCES
Volume 5, Issue 4, Pages 2684-2688Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ra13397h
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Funding
- Swedish Research Council
- Royal Institute of Technology
- People Programme (Marie Curie Actions) of the European Union's Seventh Framework Programme (FP7) under REA grant [264645]
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Isotopically pure [D-6]-dimethyl-2,2'-bipyridine derivatives were selectively and rapidly formed using microwave-assisted regioselective deuteration of the methyl moieties of the parent bipyridine in a deuterium oxide solution. For instance, [D-6]-4,4'-dimethyl-2,2'-bipyridine was formed in quantitative yield within 15 minutes, in a simple and convenient process.
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